Scanning Electron Microscope Laboratory

The Quanta 200 Environmental Scanning Electron Microscope(ESEM) from FEI Company is a special type of high performance scanning electron microscope (SEM). The instrument can be used in high vacuum mode (HV, <6×10-4Pa), low-vacuum mode (LV, 10~130Pa) and the so called ESEM (Environmental SEM) mode (10~2600Pa) with the Everhart Thornley Detector (ETD), Large Field Detector (LFD), and gaseous secondary electron detector (GSED) respectively. This makes it possible to study samples in a wide range. The highest resolution is 3.0nm (at 30 kV) and the highest magnification is 150, 000. The microscope is equipped with digital image capture and analytical systems, such as electron backscatter diffraction (with Backscattered Electron Detector, BSED) and energy dispersive spectrometer (EDS, GENESIS XM2, from EDAX Company). Qualitative and quantitative analysis, elemental mapping and line scans can be performed with the EDS. And the comprehensive and powerful, yet easy to use, microanalysis application software Genesis XM2 system together with the standard sample assemblages, allowing the materials characterization analyst to obtain the most accurate microanalysis data. The SEM system also equipped with a peltier stage (-5℃) for studies of wet samples in-situ.

Instrument data

Resolution

• High-vacuum
- 3.0nm at 30kV (SE)
- 4.0nm at 30kV (BSE)
- 10nm at 3kV (SE)
• Low-vacuum
- 3.0nm at 30kV (SE)
- 4.0nm at 30kV (BSE)
- < 12nm at 3kV (SE)
• Extended vacuum mode (ESEM)
- 3.0nm at 30kV (SE)
• Accelerating voltage: 200V – 30kV
• Probe current: up to 2μA –
continuously adjustable

Chamber

• 284mm left to right
• 10mm analytical WD
• 8 ports
• EDX take-off angle: 25°
4-axis motorized stage
• Eucentric goniometer stage
• X,Y = 50mm
• Z = 50mm (25mm motorised)
• T = -15° to +75° (manual)
• R = 360° continuous
• Repeatability: 2μm
Image processor
• Up to 4096 x 3536 pixels
• File type: TIFF (8- or 16-bit), BMPor JPEG

Advantages

• can accommodate different samples with high resolution by high- , low- and extended low-vacuum (ESEM) mode
• have all the information from the different detectors instantly available on one single screen in Quanta’s four Quadrant user interface
• low- and ESEM-vacuum capability enables charge free imaging and analysis of non-conductive specimens and/or hydrated specimens
• the EDS provides element analysis from 5B to 92U
• can perform in-situ dynamic experiments and live record them on video